<p dir="ltr">STL 3D print files for LED arc array holders for in-situ photocrystallography studies, designed to be mounted onto a 4-circle X-ray diffractometer to enable in-situ illumination of single-crystals at the same time as X-ray diffraction data is collected.</p><p dir="ltr">Examples of how to use this equipment to perform photocrystallography studies can be found in recently published research articles by the group including: </p><ol><li>Coulson and Hatcher, <b><i>CrystEngComm</i></b>, 2022, <b>24</b>, 3701-3714. doi.org/10.1039/D2CE00213B.</li><li>Morris, Coulson, Hatcher <i>et al.</i>, <b><i>Angewandte Chemie International Edition</i></b>, 2024, <b>63</b>(20), e202401552. doi.org/10.1002/anie.202401552.</li></ol><p dir="ltr">Files available:</p><ul><li>4x5mm_LED_clip.stl provides the geometry to mount 4 x 5 mm through-hole LEDs at a distance of approx. 1 cm away from the diffractometer sample position</li><li>6x3mm_LED_clip.stl provides the geometry to mount 6 x 3 mm through-hole LEDs at a distance of approx. 1 cm away from the diffractometer sample position</li><li>LED_magnetic_cryo_clip.stl provides the geometry for the clips used to attach the LED holders to the liquid nitrogen flow device</li></ul><p dir="ltr"><br></p>
Funding
URF\R1\191104
History
Data file formats
stl
Specialist software required to view data files
Any 3D printing sofware including freely available online platforms e.g. Tinkercad