STL 3D print files for LED arc array holders for in-situ photocrystallography studies, designed to be mounted onto a 4-circle X-ray diffractometer to enable in-situ illumination of single-crystals at the same time as X-ray diffraction data is collected.
Examples of how to use this equipment to perform photocrystallography studies can be found in recently published research articles by the group including:
Coulson and Hatcher, CrystEngComm, 2022, 24, 3701-3714. doi.org/10.1039/D2CE00213B.
Morris, Coulson, Hatcher et al., Angewandte Chemie International Edition, 2024, 63(20), e202401552. doi.org/10.1002/anie.202401552.
Files available:
4x5mm_LED_clip.stl provides the geometry to mount 4 x 5 mm through-hole LEDs at a distance of approx. 1 cm away from the diffractometer sample position
6x3mm_LED_clip.stl provides the geometry to mount 6 x 3 mm through-hole LEDs at a distance of approx. 1 cm away from the diffractometer sample position
LED_magnetic_cryo_clip.stl provides the geometry for the clips used to attach the LED holders to the liquid nitrogen flow device
Funding
URF\R1\191104
History
Data file formats
stl
Specialist software required to view data files
Any 3D printing sofware including freely available online platforms e.g. Tinkercad